样品分析报告
色谱柱:BBH-2560 最高使用温度:260/280℃
柱长:100m 内径:0.25mm 膜厚:0.25μm
色谱条件:
柱 温:140℃(6min)to 240℃(10min)at 2℃/min 汽化温度:220 ℃
检 测 器:FID 检测温度:230 ℃
柱前压:26.1psi 分 流 比:20:1
进 样 量:0.6uL
样品:37种脂肪酸甲酯混标
峰序 | 组分名 | 保留时间[min] | 峰面积[pA*s] | 分离度 | 拖尾因子 |
1 | 溶剂 | 13.027 | 745633.64 | 0.000 | 1.425 |
2 | C4:0 | 13.632 | 207.21 | 7.280 | 1.037 |
3 | C6:0 | 14.271 | 268.03 | 7.262 | 1.060 |
4 | c8:0 | 15.390 | 286.26 | 12.253 | 1.012 |
5 | c10:0 | 17.316 | 308.26 | 19.918 | 0.992 |
6 | c11:0 | 18.688 | 156.68 | 13.350 | 0.990 |
7 | c12:0 | 20.381 | 321.25 | 15.747 | 0.970 |
8 | c13:0 | 22.392 | 163.09 | 17.798 | 1.000 |
9 | c14:0 | 24.717 | 324.81 | 19.563 | 0.949 |
10 | C14:1 | 27.058 | 160.65 | 18.896 | 0.982 |
11 | C15:0 | 27.289 | 160.25 | 1.852 | 0.995 |
12 | C15:1 | 29.801 | 160.17 | 19.690 | 0.976 |
13 | C16:0 | 30.089 | 505.69 | 2.168 | 0.854 |
14 | C16:1 | 32.252 | 161.29 | 16.125 | 0.973 |
15 | C17:0 | 32.967 | 164.72 | 5.328 | 0.945 |
16 | C17:1 | 35.183 | 164.31 | 16.411 | 0.973 |
17 | C18:0 | 35.956 | 336.10 | 5.586 | 0.848 |
18 | C18:1n9t | 37.158 | 161.89 | 8.650 | 0.937 |
19 | C18:1n9c | 37.882 | 330.41 | 5.221 | 0.894 |
20 | C18:2n6t | 39.130 | 159.50 | 8.983 | 0.967 |
21 | C18:2n6c | 40.831 | 142.61 | 12.359 | 0.962 |
22 | C20:0 | 41.916 | 344.76 | 7.373 | 0.801 |
23 | C18:3n6 | 43.095 | 128.77 | 7.926 | 0.970 |
24 | C20:1 | 43.714 | 172.18 | 4.402 | 0.922 |
25 | C18:3n3 | 44.261 | 125.84 | 3.953 | 0.993 |
26 | C21:0 | 44.807 | 170.11 | 3.864 | 0.860 |
27 | C20:2 | 46.557 | 153.56 | 12.264 | 0.974 |
28 | C22:0 | 47.721 | 337.16 | 7.426 | 0.742 |
29 | C20:3n6 | 48.718 | 143.39 | 6.337 | 0.974 |
30 | C22:1n9 | 49.379 | 170.04 | 4.683 | 0.888 |
31 | C20:3n3 | 49.815 | 145.97 | 3.021 | 0.948 |
32 | C24:4n6 | 50.373 | 134.52 | 3.790 | 1.019 |
33 | C23:0 | 50.485 | 159.30 | 0.770 | 0.824 |
34 | C22:2 | 52.037 | 141.08 | 10.768 | 0.935 |
35 | C24:0 | 53.257 | 359.03 | 7.157 | 0.700 |
36 | C20:5n3 | 53.766 | 104.99 | 2.964 | 0.995 |
37 | C24:1 | 54.786 | 168.08 | 6.930 | 0.838 |
38 | C22:6n3 | 60.814 | 81.96 | 38.450 | 1.013 |
37种脂肪酸甲酯混标3针重复性谱图及结果